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  • Dr. Kali Sanjay, Scientist-G - Head 9338291970,   ksanjay.immt@csir.res.in ,  

    DESCRIPTION :

    Dr. Kali Sanjay, Chief Scientist at the Council of Scientific and Industrial Research’s Institute of Minerals and Materials Technology, Bhubaneswar, India, leads the Hydro, Bio & Electrometallurgy Department, Business Development, and the Centre of Excellence on Critical Minerals under the National Critical Mineral Mission of the Ministry of Mines. With over three decades of experience, he specialises in developing technologies for recovering critical metals from ores, wastes and secondary resources. He has authored 60+ research publications, holds 7 patents, and contributed to 100 research and technology projects, resulting in 17 technologies and processes. He serves on Indian national bodies, including committees on Critical and Strategic Minerals and Nickel and Cobalt, and chairs a Bureau of Indian Standards committee on aluminium-industry feedstocks. His international engagements span Australia, Canada, South Korea and Europe. He is a Professor at the Academy of Scientific and Innovative Research, advancing sustainable resource security.

    EXPERIENCE :
    • 1993 to 1998 Jr. Scientist.
    • 1998 to 2002 Scientist.
    • 2002 to 2006 Sr. Scientist.
    • 2006 to 2012 Principal Scientist.
    • 2012 to 2017 Sr. Principal Scientist.
    • 2017 to continuing Chief Scientist (Scientist G)
    AREA OF INTEREST :

    Design and scale-up of hydrometallurgical unit operations

    Process flow-sheet development to recover non-ferrous metals from low-grade ores/secondaries.

    Solid wastes and effluents processing / electroremediation / electrowashing / salt-splitting.

    Development of technologies for critical minerals.

    AWARDS & HONOURS :

    Received fourth prize (Rs One lakh prize) in the ‘Grand fly ash utilisation challenge’ contest conducted by NTPC during 2018-19.

    NESA Fellowship of the Year Award 2021 during 2021-22.

    Eminent Engineering Personality Award by The Institution of Engineers India (IEI) during 2022- 23.

    RECENT PUBLICATIONS :

    Books / Book chapters

    1.     ‘Polymetallic Nodules’; Proceedings of National Seminar on Polymetallic Nodules, Editors: Shashi Anand and Kali Sanjay, 2005.

    2.     Book chapter on ‘Aqueous Electrodeposition of Non-Ferrous Metals,’ Tondepu Subbaiah and Kali Sanjay in ‘Electrodeposition: Properties, Processes, and Applications,’ Nova Science Publishers, Inc. ISBN-10: 1614708266 & ISBN-13: 978-1614708261, 2011.

    3.     Book chapter on ‘Arsenic Removal from Industrial Effluents through Ferric Arsenate Precipitation’ in ‘Environmental Science and Engineering, Vol. 4: Water Pollution & Waste Water Treatment,’ Barsha Dash, Geetanjali Mishra, Kali Sanjay, and Tondepu Subbaiah, Pages 354-363, Editor of Volume Dr. J C Singhal, Chief Editor Dr. Bhola R Gurjar, Executive Editor Dr. J.N. Govil, Publisher Studium Press LLC, USA, ISBN of Series 1- 62699-088-3, ISBN of Volume 1-62699-092-, 2017.

    4.     Book Chapter on ‘Kaolin: An Alternate Resource of Alumina’ in ‘Sustainable Chemical, Mineral, and Material Processing. Lecture Notes in Mechanical Engineering,’ Routray, S., Dash, B., Sheik, A.R., Sarangi, C.K., Sanjay, K., Editor Chinthapudi, E., Basu, S., Thorat, B.N., Springer, Singapore. https://doi.org/10.1007/978-981-19-7264-5_10, 135-144, 2022.

    5.     Book Chapter on ‘Considerations for Using Polymetallic Nodules as Alternative Metal Extraction Resource: Focus on Energy-Related Applications’ in ‘Deep-Sea Mining and the Water Column,’ P. K. Sen and K. Sanjay, Editor Rahul Sharma. Cham: Springer Nature Switzerland. https://doi.org/10.1007/978-3-031-59060-3_5, 129-164, 2024.

    Recent Publications (https://scholar.google.co.in/citations?user=3MhEeZAAAAAJ&hl=en)

    1.Extraction and recovery of V (V) from citrate leachate of spent catalyst containing impurities (Mg and Fe) using tricapryl methyl ammonium chloride, Adyasha Swain Mohapatra, Chinmaya Kumar Mohanty, Kali Sanjay, Pankaj Kumar Parhi, Hydrometallurgy, Doi 10.1016/j.hydromet.2026.106798, June, 2026

    2.Electrochemically activated intermetallic enriched polymetallic nodules for sustainable oxygen evolution electrocatalysis; S Mariappan, R Kiran, S Sharmila, Kali Sanjay, D Kalpana., Journal of Power Sources, Vol 677, 239982, 15 June 2026.

    3.Optimization of organic acids and organophosphorus extractants for sustainable and selective recovery of rare earth elements from waste permanent magnets of wind turbines. Prasanjit Das, Abdul Rauf Sheik, Kali Sanjay, Niharbala Devi. Journal of Rare Earths, Available online March, 2026, https://doi.org/10.1016/j.jre.2026.03.013.

    4.Comparative Leaching of Rare Earth Elements from Roasted and Unroasted End‐of‐Life HDDs Magnet and Kinetic Study Using Hydrochloric Acid. Prasanjit Das, Abdul Rauf Sheik, Kali Sanjay, Niharbala Devi. Environmental Quality Management, Vol 35, no 2 p e70244, December, 2025. 

    5.Liquid-liquid extraction of Nd (III) using [P66614][Cy272] ionic liquid. Das Prasanjit, Kali Sanjay, Devi Niharbala. Journal of Metals, Materials and Minerals Vol. 35. No. 2 p e2252-e2252, Aug. 2025.

    6.Solvoleaching Approach for SmCo5 Alloy Scrap and Production of Sodium Samarium Sulfate and Cobalt Oxide. Prasanjit Das, Binapani Behera, Kali Sanjay, Niharbala Devi.  Journal of Alloys and Compounds Volume 1035, p 181469, 5 July 2025.

    7.Graphitic carbon nitride loaded Bi4O5I2 for elevated photocatalytic tetracycline degradation. Subhasish Mishra, Barsha Marandi, Kali Sanjay, Rashmi Acharya, J Met Mater Miner, vol. 35, no. 2, p. e2261, May 2025.

    8.A Novel Process for Preparing Aluminium Fluoride from Coal Fly Ash Using Hydrofluorosilicic Acid Leaching and Seeding Techniques. Tripathy, Anil Kumar, Sayani Adhikari, Bankim C. Tripathy, Kali Sanjay, and Indra N. Bhattacharya. Journal of Sustainable Metallurgy, 1-13, 2025.

    9.Recovery of iron as hematite and separation of trivalent lanthanide ions from spent hard disk magnet leach liquor using [P66614][Cy272] ionic liquid. Prasanjit Das, Binapani Behera, Kali Sanjay, and Niharbala Devi. RSC Advances, Volume 15(2), 912-923, 2025.

    10.Designing g-C3N4/NiFe2O4 S-scheme heterojunctions for efficient photocatalytic degradation of Rhodamine B and tetracycline hydrochloride. Subhasish Mishra, Lopamudra Acharya, S Sharmila, Kali Sanjay, and Rashmi Acharya. Applied Surface Science Advances, Volume 24, 100647, 2024.

    11.Liquid-liquid extraction and separation of light and heavy rare earth elements from chloride solution using a mixture of tertiary amine and phosphinic acid: recycling strategies for NdFeB magnet. Prasanjit Das, Abdul Rauf Sheik, Kali Sanjay, and Niharbala Devi. Geosystem Engineering, 1-11, 2024.

    12.Insight into Cu Extraction Using Deep Eutectic Solvent: Reaction Mechanism. Sonidarsani Routray, Binapani Behera, Barsha Marandi, K. Sanjay, M. K. Ghosh, and Barsha Dash.  Metallurgical and Materials Transactions B, 1-8, 2024.

    13.Anoxic Manganese Bioleaching–Investigation of Scale-up Parameters in a Stirred Bioreactor. Tejaswini Das, V. Aishvarya, N. Pradhan, K. Sanjay. Geomicrobiology Journal, 41(9), 939-946, 2024.

    14.Boosted photocatalytic accomplishment of 3D/2D hierarchical structured Bi4O5I2/g-C3N4 pn type direct Z-scheme heterojunction towards synchronous elimination of Cr (VI) and tetracycline. Subhasish Mishra, Lopamudra Acharya, Barsha Marandi, Kali Sanjay, and Rashmi Acharya. Diamond and Related Materials, Volume 142, 110834, 2024.

    15.Recovery of Tellurium from Waste Anode Slime Containing High Copper and High Tellurium of Copper Refineries. Sarangi, Chinmaya Kumar, Abdul Rauf Sheik, Barsha Marandi, Vijetha Ponnam, Malay Kumar Ghosh, Kali Sanjay, Manickam Minakshi, and Tondepu Subbaiah. Sustainability, no. 15, 11919, 2023.

    16.Towards Solving the Complexity Associated with Continuous Countercurrent Decantation (CCD) System in Solid-Liquid Separation Processes. Tripathy, A.K., Behera, S.S., Marandi, B., Sahu, P., Sheik, A.R., Aishvarya, V., Bhattacharya, I.N. and Sanjay, K., Journal of The Institution of Engineers (India): Series D, Volume 105, pages 1223–1229, 2024.

    17.High pure Co(II) precursor liquor from spent catalyst leach liquor. R Samal, S Mahalik, S Routroy, K Sanjay, B Dash, Journal of Sustainable Metallurgy, Volume 9, pages 972–981, 2023.

    18.Photocatalytic degradation of malachite green using TiO2 and ZnO impregnated on fecal sludge derived biochar. N Tiwari, S Chakrabortty, K Samal, S Moulick, BG Mohapatra, S Samanta, PK Mohapatra, K Sanjay, J Nayak, S Banerjee, SK Tripathy, Journal of the Taiwan Institute of Chemical Engineers, Volume 145, 104800, 2023.

    19.Extensive investigation on extraction behaviour of organo-phosphrous based bi-functional ionic liquids for separation of molybdenum (Mo) from spent Co-Mo/Al2O3 leach liquor. S Mohapatra, SS Behera, S Tripathy, PK Parhi, K Sanjay, Journal of Molecular Liquids, Volume 366, 120087, 2022.

    20.Facile synthesis, characterization and application of magnetic Fe3O4-coir pith composites for the removal of methyl violet from aqueous solution: Kinetics, isotherm, thermodynamics and parametric optimization. Sanjay Sarkar, Nitika Tiwari, Meerambika Behera, Sankha Chakrabortty, Kavya Jhingran, Kali Sanjay, Shirsendu Banerjee, Suraj K. Tripathy, Journal of the Indian Chemical Society, Volume 99, Issue 5, 100447, 2002.

    21.Reclamation of tungsten from spent HDS catalyst: a detailed study, Mahalik, Surjeet, A. R. Sheik, Barsha Dash, C. K. Sarangi, and K. Sanjay, Indian Chemical Engineer Pages 416-429, 2022.

    22.Ionic mass transfer at point electrodes located at cathode support plate in an electrorefining cell in presence of rectangular turbulent promoters, Subbaiah, T., P. Vijetha, B. Marandi, K. Sanjay, and M. Minakshi., Sustainability 14, no. 2 , 880, 2022.

    23.Recovery of Lead as Lead Sulphide from Anode Slime Using Hydrometallurgical Technique, Mishra, G., B. Dash, A. R. Sheik, C. K. Sarangi, P. Vijetha, K. Sanjay, M. K. Ghosh, and T. Subbaiah., Journal of The Institution of Engineers (India): Series D 102, no. 2 489-494, 2021.

    24.Citric acid mediated leaching kinetics study and comprehensive investigation on extraction of vanadium (V) from the spent catalyst, Mohanty, C., S. S. Behera, B. Marandi, S. K. Tripathy, P. K. Parhi, and K. Sanjay, Separation and Purification Technology 276, 119377, 2021.

    25.Sorptive removal of malachite green from aqueous solution by magnetite/coir pith supported sodium alginate beads: Kinetics, isotherms, thermodynamics and parametric optimization, Sanjay Sarkar, Nitika Tiwari, Aradhana Basu, Meerambika Behera, Bhaskar Das, Sankha Chakrabortty, Kali Sanjay, Mrutyunjay Suar, Tapan Kumar Adhya, Shirsendu Banerjee, Suraj K Tripathy, Environmental Technology & Innovation, Volume 24, 101818, 2021

    26.Manganese enrichment of polymetallic oceanic nodules via selective leaching process for energy storage applications, Priyanka Mukherjee, Sushree Pattnaik, Kali Sanjay, Mamata Mohapatra, Journal of Chemical Technology & Biotechnology, Vol 96(5), 1246-1257, 2021

    27.Synthesis of iron molybdate from molybdenum spent catalyst and evaluation of its electrochemical properties, Rasmita Barik, Priyanka Mukherjee, Kishor Kumar Sahu, Kali Sanjay, Malay Kumar Ghosh, Mamata Mohapatra, Environmental Progress & Sustainable Energy, Vol 40 (3), 13560, 2021.

    28.An anionic and cationic surfactant-assisted hydrothermal synthesis of cobalt oxide nanoparticles as the active electrode material for supercapacitors, RR Samal, Aneeya K Samantara, S Mahalik, JN Behera, B Dash, K Sanjay, New Journal of Chemistry, Vol 45 (5), 2795-2803, 2021.

    29.Solvent Extraction of Copper Enhanced by Mixing Cavities in Micromixer, Abdul Rauf Sheik, Amol A Kulkarni, Kali Sanjay, Solvent Extraction Research and Development, Japan, Vol 28 (1), 37-47, 2021.

    30.Unravelling for 1st time electrochemical sensing of As (III) by 3D cavitized kagome type lattice, Priyanka Mukherjee, Benjamin Raj, Arun Kumar Padhy, Kali Sanjay,  Suddhasatwa Basu, Mamata Mohapatra, Journal of Electroanalytical Chemistry, Volume 877, 114725, 15 November 2020.

    31.Leaching of Rare Earth Elements from the Residue Generated by the Lixiviation of Waste Phosphor with Sulphuric Acid, A Anand, R Singh, J Samantray, MK Ghosh, K Sanjay, Transactions of the Indian Institute of Metals,1-11, 2020.

    32.A pyro-hydrometallurgical process for the recovery of alumina from waste aluminium dross, A K Tripathy, S Mahalik, C K Sarangi, B C Tripathy, K Sanjay, IN Bhattacharya, Minerals Engineering, Vol 137, 181-186, 2019.

    33.Sodium fluoride assisted acid leaching of coal fly ash for the extraction of alumina, AK Tripathy, B Behera, V Aishvarya, A R Sheik, B Dash, C K Sarangi, B C Tripathy, K Sanjay, I N Bhattacharya, Minerals Engineering, Vol 131, 140-145, 2019.

    34.Raman analysis of the formation of dithionate during copper electrowinning, Tondepu Subbaiah, Chinmaya Kumar Sarangi, Kali Sanjay, Manickam Minakshi Sundaram, World of Metallurgy – ERZMETALL, Vol. 71, Issue. 2, 92-98, 2019.

    35.Leaching and Preparation of Co-Mo Sulfide/Oxide Nanoparticles from Spent Catalyst, Mamata Mohapatra, Suchismita Sahu, Rasmita Barik, Eliza Padhan, Priyanka Mukherjee, Mahasweta Moharana, Alfara A. Baba, Kali Sanjay, JOM, Vol. 70, No. 10, 1-7, 2018.

    36.Factorial design for process optimization and generation of kinetic data for yttrium and europium leaching, Amit Anand, Randhir Singh, Malay Kumar Ghosh, Kali Sanjay, Mineral Processing and Extractive Metallurgy, 1-9, 2018.

    37.Recovery of dimethylglyoxime (DMG) from Ni-DMG complexes, Meenakshi Rath, Laxmi Priya Behera, Barsha Dash, Abdul Rauf Sheik, Kali Sanjay, Hydrometallurgy, Vol 176, 229–234, 2018.

    38.Influence of synthesis temperature on the growth and surface morphology of Co3O4 Nanocubes for supercapacitor applications, Rashmirekha Samal, Barsha Dash, Chinmaya Kumar Sarangi, Kali Sanjay, Tondepu Subbaiah, Gamini Senanayake, Manickam Minakshi, Nanomaterials, Vol 7(11), 356, 2017.

    39.Electrochemical fencing of Cr (VI) from industrial wastes to mitigate ground water contamination, N Shukla, MK Harbola, K Sanjay, R Shekhar, Transactions of the Indian Institute of Metals, Vol 70 (2), 511-518, 2017.

    40.Branched Platinum Nanostructures on Reduced Graphene: An excellent Transducer for Nonenzymatic Sensing of Hydrogen Peroxide and Biosensing of Xanthine, Tapan Kumar Behera, Subash Chandra Sahu, Biswarup Satpati, Bamaprasad Bag, Kali Sanjay, Bikash Kumar Jena, Electrochimica Acta, Vol 206, 238–245, 2016.

    41.Processing Nigerian pyrolusite ore, Part I: Characterization and dissolution kinetics analysis, A. A. Baba, L. Ibrahim, R. B. Bale, A. G. F. Alabi, F. A. Adekola, M. K. Ghosh, K. Sanjay, and A. R. Sheik, Canadian Institute of Mining, Metallurgy and Petroleum Journal, Vol 7(1), 43-51, 2016.

    42.Micellar mediated selective leaching of manganese nodule in high temperature sulfuric acid medium, R. Barik, K. Sanjay, B.K. Mishra, M. Mohapatra, Hydrometallurgy, Vol 165(1), 44–50, 2016.

    43.Reactor and column leaching studies for extraction of copper from two low grade resources: A comparative study, Sandeep Panda, Geetanjali Mishra, Chinmaya Kumar Sarangi, Kali Sanjay, Tondepu Subbaiah, Subir Kumar Das, Kadambini Sarangi, Malay Kumar Ghosh, Nilotpala Pradhan, Barada Kanta Mishra, Hydrometallurgy, Vol 165(1), 111–117, 2016.

    44.Electrolytic manganese dioxide (EMD): a perspective on worldwide production, reserves and its role in electrochemistry, Avijit Biswal, Bankim Chandra Tripathy, Kali Sanjay, Tondepu Subbaiah and Manickam Minakshi, RSC Adv., 5, 58255–58283, 2015.

    45.Aluminium recovery from NALCO fly ash by acid digestion in the presence of fluoride ion, A.K. Tripathy,C.K. Sarangi, B.C. Tripathy, K. Sanjay, I.N. Bhattacharya, B.K. Mahapatra, P.K. Behera, B.K. Satpathy, International Journal of Mineral Processing, Vol 138, 44–48, 10 May 2015.

    46.Recovery of Co metal and Electrolytic Manganese Dioxide (EMD) from Co–Mn sludge, A. Biswal, S. Mahakud, Sandhyarani Bhuyan, B. Dash, C.K. Sarangi, Kali Sanjay, B.C. Tripathy, T. Subbaiah, I.N. Bhattacharya, Sung-Ho Joo, Shun Myung Shin, K.H. Park, Hydrometallurgy, Vol 152, 159–168, 2015.

    47.Ligand mediated eco-friendly leaching of zinc from spent catalyst in alkaline media, M. Mohapatra, Banaja Nayak, K. Sanjay, T. Subbaiah, B.K. Mishra, Journal of Industrial and Engineering Chemistry, Vol 20, Issue 4, 2217–2223, 2014.

    48.Electro-crystallization of Antimony from Acidic and Alkaline Baths in Diaphragm-less Cell, Chinmaya Kumar Sarangi, Ayonbala Baral, Jayasmita Panigrahi, Kali Sanjay, Tondepu Subbaiah, Barada Kanta Mishra, Advanced Materials Research, Vol. 828, 65- 72, 2014.

    49.Behaviour of arsenic(III) and antimony(III) during electrowinning of nickel from aqueous sulphate solutions; R.R. Samal, C.K. Sarangi, B.C. Tripathy, K. Sanjay, I.N. Bhattacharya, T. Subbaiah., Hydrometallurgy, Vol. 139, 39-45, 2013.

    50.Aqueous processing of nickel spent catalyst for a value added product; Sheik, A.R., Ghosh, M.K., Sanjay, K., Subbaiah, T., Mishra, B.K., Baba, A.A.; Korean Journal of Chemical Engineering, Vol. 30 (2), 400-404, 2013.

    51.Extraction of Cu and Cr from a spent Cu–Cr catalyst: Recovery enhancement through mechanical activation; Swaroopa, S., Ghosh, M. K., Sanjay, K. and Mishra, B. K. Hydrometallurgy, Vol. 136, 8–14, 2013.

    52.Extraction of Ni (II) from Spent Hydrodesulfurization HDS Catalyst Through Leaching and Electroless Precipitation of Ni(OH)2., Pradhan, S.R., Dash, B., Sanjay, K., Subbaiah, T. Metallurgical and Materials Transactions B: Process Metallurgy and Materials Processing Science, Vol. 44(2), 469-476, 2013.

    53.Dissolution kinetics of nickel from spent catalyst in nitric acid medium. Sheik, A.R., Ghosh, M.K., Sanjay, K., Subbaiah, T., Mishra, B.K. Journal of the Taiwan Institute of Chemical Engineers, Vol. 44, Issue 1, 34-39, 2013.

    54.Influence of the microstructure and its stability on the electrochemical properties of EMD produced from a range of precursors, A Biswal, BC Tripathy, K Sanjay, D Meyrick, T Subbaiah, M Minakshi, Journal of Solid State Electrochemistry 17 (12), 3191-3198, 2013.

    55.Influence of alternative alkali reagents on Fe removal during recovery of Mn as Electrolytic Manganese Dioxide (EMD) from Mn sludge, Avijit Biswal, Barsha Dash, BC Tripathy, T Subbaiah, Shun Myung Shin, Kali Sanjay, BK Mishra, Hydrometallurgy 140, 151-162, 2013.

    56.Insights into heap bioleaching of low grade chalcopyrite ores — A pilot scale study., S. Panda, K. Sanjay, L.B. Sukla, N. Pradhan, T. Subbaiah, B.K. Mishra, M.S.R. Prasad,

    57.        S.K. Ray., Hydrometallurgy., Vol. 125-126., 157-165, 2012.

    58.Electrokinetic cleaning of industrial residues; Sanjay, K., Shekhar, R.; Transactions of the Institutions of Mining and Metallurgy, Section C: Mineral Processing and Extractive Metallurgy, Vol 121 (2), 117-120, 2012.

    59.Electroosmotic pump: Rate controlling mechanism for unusually fast electroremediation kinetics of Cr(VI) in basic Kanpur soil; Sanjay Kali, R.P. Das, Rajiv Shekhar; Electrochimica Acta, Vol 86, 80-88, 2012.

    PATENTS :

    International

    A process for extraction of nickel from low-grade chromite ore (International Patent Numbers: European Patent (EP1697549 B1); Australian Patent (AU 2002348824 B2); Indian patent (234452 (0483/DEL/2003)).

    An electrochemical system and process for the reduction of nitric acid concentration using electrolytic cell (Patent File No. 3198/DEL/2012; US 20150291451 A1; WO 2014057505 A4).

    Hydrometallurgical process for the recovery of tellurium from high lead-bearing copper refinery anode slime. (Paten File No: 2459DEL2013; US Patent App. US20150053572 A1).

     

     Indian

    A process for production of crystalline boehmite by precipitating from supersaturated sodium aluminate liquor under atmospheric conditions at a temperature as low as 500C (Patent No. 267384 Dated 28/07/2015).

    An improved process for the continuous conversion of Fe (III) present in phosphoric acid to Fe(II) by electrolytic reduction  (Patent File No.0063/DEL/2008).

    A pyro-hydrometallurgical process for the recovery of alumina and calcium silicate from flyash (Patent File No: 0252NF2015)

    PROJECTS WORKED ON :

    Research Projects

    Projects completed as Project Leader

    1.  ‘Detailed Engineering Design of Solvent Extraction – Electrowinning for extraction of cobalt from super alloy scraps: 200 kg/day capacity’. M/s Rubamin Ltd., Baroda.

    2.  ‘Modelling of the electrorefining cell in the pyroprocessing demonstration facility’, IGCAR (DAE), Kalpakkam.

    3.  ‘Development of electrochemical mixer-settler and optimization studies for the recovery of palladium from high-level liquid waste’, IGCAR (DAE), Kalpakkam.

    4.  ‘Extraction of Tungsten values from Hutti gold mine tailings concentrate and scrap: process flow sheet development, bench scale studies and pilot scale testing’; Defense Metallurgical Research Laboratory (DRDO), Hyderabad.

    5.  ‘Recovery of alumina from Fly ash – modifications and validation of flow sheet’; National Aluminium Company Ltd. (NALCO), Bhubaneswar.

    6.  ‘Recovery of Electrolytic Manganese Dioxide (EMD) from Manganese Ore: Process optimization for existing plant at MOIL, alternate process development and Basic Engineering Package preparation’; Manganese Ore India Ltd. (MOIL), Nagpur.

    7.  ‘Technology transfer of cobalt manufacture’; Mishra Dhatu Nigam Limited, (MIDHANI), Hyderabad.

    8.  ‘Evaluation of suitability of Nano iron/ iron oxide powders for energy and sensor applications’; National Minerals Development Corporation (NMDC), Hyderabad.

    9.  ‘Cobalt technology from impure cobalt hydroxide: Process flow sheet development’; Mishra Dhatu Nigam Limited (MIDHANI), Hyderabad.

    10. ‘Technology development, demonstration and shifting of 1000 cm2 EM cell for splitting of sodium sulphate solution to sodium hydroxide and sulphuric acid’; Heavy Water Board, Mumbai.

    11. ‘Electroremediation of soils contaminated with heavy metals / organic pollutants and radio nuclides’, CSIR Taskforce.

    12. ‘Waste to wealth through Hydro & Electrometallurgical processing’, CSIR Non-network project.

    13. ‘Engineering consultancy work for development of Electrolytic – Membrane process for conversion of effluent sodium sulphate solution to sodium hydroxide and sulphuric acid‘; HWB (DAE), Mumbai.

    14. ‘Multifunctional electrodes and electrolytes for futuristic electrochemical technologies’; CSIR XII plan (CSC0101), New Delhi.

    15. ‘Feasibility studies to recover Mn metal from low grade Mn ore’; TATA Steel Ltd., Jamshedpur.

    16. ‘Process scale-up and feasibility study for improving Mn/Fe ratio of low grade manganese ore’; TATA Steel Ltd., Jamshedpur.

    17. ‘Evaluation of design parameters for dewatering of manganese nodules’; National Institute of Ocean Technology (NIOT), Chennai.

    18. ‘Recovery of alumina from Fly ash’; CSIR (FTT Project).

    19. ‘Technology Development for holistic utilization of Red Mud’; HINDALCO, NALCO and VEDANTA.

    20. ‘Process development and bench scale testing for recovery of Lithium and Cobalt from spent Lithium batteries’; Excel Industries Ltd. Mumbai.

    21. ‘Recovery of copper from copper oxide ore’; Onshore Construction Company Pvt. Ltd., Mumbai

    22.    ‘Feasibility Studies for Preparation of Fused Magnesia from Kimberlite Tailings’; NMDC Hyderabad.

    23. ‘Titanium dioxide recovery and waste management from vanadiferrous titano-magnetite and ilmenite concentrates’; Commonwealth Scientific and Industrial Research Organisation (CSIRO) Australia.

    24. ‘Upscaling of Nd metal/Nd-Pr production along with other rare earth metals (La,Ce) and their alloys by Molten Salt Electrolysis routes (Phase I)’; CSIR, New Delhi

    25. ‘Scale-up study of electrolysis of Cuprous chloride (Phase I)’; ONGC Energy Center, Mumbai.

     

    Ongoing projects

     

    26. ‘Technology development (Extractive metallurgy) for Polymetallic nodules (PMN)’ (Project Leader); Ministry of Earth Sciences, Govt. of India.

    27. ‘Advanced recovery of the battery materials and REE from ores and wastes’ (AISRF Round 14) (Project Leader); Indo-Australian Project, Department of Science & Technology, Govt. of India.

    28. ‘Setting up of pilot cum demonstration plant for recovery of alumina and value-added products from fly ash’ (Project Leader); Ministry of Mines, NALCO & CSIR.

    29. Characterisation and Feasibility of Recovering Trace and Rare Earth elements from Coal/Fly Ash /bottom ash, Shale, Clay, Sandstone, and Granite Rocks, (Project Leader); Singareni Collieries Company Ltd.

    30. ‘Process design for Se, Te, Cu Recovery’ (Co-Project Leader); Sterlite copper, Silvassa plant, A unit of Vedanta Ltd, Silvassa.

    31. ‘Plant Audit of MALCO Energy Limited-Nickel Business Unit’ (Co-Project Leader); MALCO Energy Limited (MEL), A unit of Vedanta Ltd, Silvassa.

    32. ‘Production of Ferro-Titanium alloy from Bauxite residue by recovery and matrix change of the metal values’; (Co-Project Leader); NALCO Bhubaneswar.

    33. ‘Shipboard-based       nodule  sieving  and       dewatering        studies  and       prototype           design development’; (Co-Project Leader); NIOT Chennai.

    34. ‘Study on breakage/ degradation of Polymetallic Nodules during vertical slurry transport through a pipe’; (Co-Project Leader); NIOT Chennai.

    35. ‘Recovery of Dehydrated Magnesium Chloride Using Sea Water Bitterns at Relatively low Temperatures in Pilot Scale’; (Co-Project Leader); CSIR.

    36. ‘Solvent Extraction (SX) Pilot Plant for REE Separation’ (Co-Project Leader); CSIR.

    37. ‘An advanced technology for improvement in alumina productivity: Scale-up testing and process validation’; (Member), Vedanta Ltd.

    38. ‘Hematite production and recovery of valuable metals from Jarosite’ (Co-Project Leader); Hindustan Zinc Ltd. Udaipur

    39. ‘Recovery of Selenium and Tellurium from anode slimes (Co-Project Leader); Sterlite copper, Silvassa plant, A unit of Vedanta Ltd, Ministry of Mines, CSIR.

    40. ‘Recovery of Copper from low-grade copper ores: oxide and sulfide ores’ (Co-Project Leader); CSIR.

    41. ‘Recovery of Co and Ni from Chromite Overburden and residue utilization’ (Co-Project Leader); CSIR.

    42. ‘Recovery of vanadium from pet coke ash, spent vanadium catalyst and vanadium concentrate’ (Co-Project Leader); CSIR.

    43. Extraction of sand and other minerals from Overburden and Carbonaceous Wastes, (Co-Project Leader); NTPC Mining Ltd.

    44. Extraction of minerals from Thermal Flyash- Phase I, (Co-Project Leader); NTPC Mining Ltd.

    45. Pilot scale testing of Process flow sheet for Preparation of Anhydrous Magnesium Chloride from Sea Water Bitterns, (Co-Project Leader); Naval Research Board (DRDO)

    Projects completed as Co-Principal Investigator (Co-PI) / Activity in-charge / Member

    46. Nickel Technology Proving Plant at RRL by GTZ- CSIR-HZL (10 tpd raw material processing ‘Technology Proving Plant’), German Agency for Technical Collaboration (GTZ), CSIR & HZL

    47. Development of process for extraction of Cu, Ni, Co & Mn from deep sea ocean nodules and testing in pilot scale (Technology Proving Plant in a scale of 500 kg/day nodules), Ministry of Earth Sciences, New Delhi

    48. Advice on processing of secondary cobalt-containing materials, M/s Rubamin Ltd, Baroda

    49. Literature survey on electrolytic nickel hydroxide, M/s Techno Chemicals, Mumbai

    50. Preparation of engineering package for a 1200 tpa nickel electrowinning plant, M/s NICOMET Ind. Ltd., Mumbai

    51. Pressure leaching of Ni-Co sulphides of M/s Nicomet Industries Ltd, M/s NICOMET Ind. Ltd. , Mumbai

    52. Development of a process for recovery of metal values from dust and sludges of Durgapur Steel Plant, RDCIS, SAIL, Ranchi

    53. Preparation of Nickel Hydroxide suitable to Nickel Cadmium and Nickel metal hydride batteries, MNES, New Delhi

    54. Solid and liquid waste inventorisation, characterization and disposal plan for the proposed second phase expansion for NALCO production and handling plants. (Smelter at ANGUL), National Aluminium Company Ltd. (NALCO), Bhubaneswar

    55. Basic study on precipitation of Boehmite, National Aluminium Company Ltd. (NALCO), Bhubaneswar

    56. Technical know-how and experimental back up for electrolytic reduction of iron (III) present in phosphoric acid to iron (II) state, Heavy Water Board (DAE)

    57. Prevention of coal dust at mechanical coal handling plant, Paradip Port Trust, Odisha

    58. Recovery of copper and tellurium from secondary raw materials, M/s Grishma Special Chemicals, Mumbai

    59. Development and design of diaphragm-less cells for electrolytic acid killing, IGCAR (DAE), Kalpakkam

    60. Recovery of copper from copper bearing slag tailings, Aditya Birla Copper, Mumbai

    61. Chromite recovery from COB plant tailings and sub grade chromite ore, Jindal Stainless Steel, Bhubaneswar.

    62. Consultancy assistance for setting up of the 500TPD commercial chromite beneficiation plant and to assist its flotation plant performance evaluation, Jindal Stainless Steel, Bhubaneswar

    63. Laboratory scale study on alumina trihydrate productivity using catalyst, National Aluminium Company Ltd. (NALCO), Bhubaneswar

    64. Collection characterization and screening of potential micro algae from West Bengal and Odisha coast and pilot scale demonstration of algal oil production, Department of Biotechnology, New Delhi

    65. Microbial desulphurization of calcined petroleum coke (Phase I & II), ALCOA, USA

    66. Laboratory testing of copper oxide ore, Oman, Engineers India Ltd., New Delhi

    67. Production of manganese sulphate from low grade manganese ore of Gujarat by non-conventional leaching techniques, Gujarat Mineral Development Corporation (GMDC), Gujarat

    68. Globally competitive chemical processes and products, CSIR taskforce project

    69. Consultancy for installation and commissioning of a commercial plant to produce 8 tpd of high pure Cu cathode through acid leaching – electrowinning route, M/s ASSM General Trading Company, UAE

    70. Recovery of nickel from chromite over burden of Orissa Mining Corporation, Orissa Mining Corporation, Bhubaneswar

    71. Detailed Design, Inspection, Testing and Commissioning of Electrolytic Reduction Cell Assembly for TDP at RCF, Trombay, Heavy Water Board (DAE), Mumbai

    72. Nickel recovery from refinery electrolyte (Phase- I&II), Hindalco Industries (Birla copper unit), Dahej.

    73. Recovery of tellurium powder from anode slimes, Hindalco Industries (Birlacopper unit), Dahej.

    74. Recovery of lead from anode slimes, Hindalco Industries (Birla copper unit), Dahej

    75. Basic engineering process package for recovery of tellurium powder and removal of lead from anode slimes, Hindalco Industries (Birla copper unit), Dahej

    76. Metallurgical test work on recovery of Cu from leach residue, M/s. Chandra Proteco Ltd., Silvassa, India

    77. Preparation of techno-economic feasibility report for 700 tpd low grade rock phosphate ore beneficiation plant for RSMML, Rajasthan, Rajasthan State Mines & Minerals Ltd., Udaipur, Rajasthan

    78. Recovery of copper from copper bearing slag tailings, Aditya Birla Copper, Mumbai

    79. Preparation and characterization of EMD suitable for batteries from slurry containing Mn and Co, KIGAM, South Korea

    80. Recycling of Lithium ion batteries, Renault Nissan Technology, Chennai

    81. An investigation on recovery of alumina in NALCO fly ash through pyro-hydrometallurgical / bioprocessing methods, National Aluminium Company Ltd. (NALCO), Bhubaneswar

    82. Electrochemical process for improving productivity of alumina in Bayer liquor, National Aluminium Company Ltd. (NALCO), Bhubaneswar.

    83. Recyclability strategy of value added utilization of iron/ manganese ore tailing /low grade ore: evaluation of energy storage capacities, Ministry of Mines, Govt. of India

    84. Processing of secondary resources for the production of battery materials, CSIR-FTT Project

    85. Manganese nodules slurry characteristics and pumping studies for vertical transport, NIOT, Chennai

    86. Multi-helical microfluidic system for integrated extraction- separation of metal ions, Department of Science and Technology (DST), Govt. of India

    87. Feasibility of bauxite leaching under high temperature conditions, HINDALCO Industries Limited, Belagavi

    88. Preparation of Basic Engineering Package (BEP) for setting up of pilot plant on use of fly ash/pond ash for production of wear resistant ceramic tiles, National Aluminium Company Ltd. (NALCO), Bhubaneswar

    89. Optimization of process for the treatment of Spent Pot Lining carbon for the recovery of valuables and bench scale testing, National Aluminium Company Ltd. (NALCO), Bhubaneswar

    90. Development of process for the production of pure and white Alumina Tri Hydrate (ATH) for solid surface application, National Aluminium Company Ltd. (NALCO), Bhubaneswar

    91. Sedimentation studies, up-scale testing and basic engineering for thickener for treatment of Mn ore fines, Manganese Ore India Limited (MOIL), Nagpur

    92. Feasibility Laboratory Studies for Liberator Cake Quality Improvement and Copper Electrowinning Process Optimisation in Cu refinery at Dahej, HINDALCO Birla Copper Unit, Dahej

    93. Electrolytic-membrane process for the production of hydrogen from seawater (Phase I: Laboratory scale optimization), ONGC Energy Centre, Mumbai

    94. Kinetic studies of different unit operations (desilication, digestion, and precipitation) of Bayer process at NALCO, National Aluminium Company Ltd. (NALCO), Bhubaneswar.

    TECHNOLOGY COMMERCIALIZED :

    Technology / Process / Know-how developed

    1.  Recovery of copper from copper oxide ore from DR Congo and providing Basic Engineering Process Package for 12000 TPA Cu extraction plant and associated cobalt, 2025, Onshore Construction Company Pvt. Ltd., Mumbai

    2.  Process development and bench scale testing for recovery of Lithium and Cobalt from spent Lithium batteries, 2025, Excel Industries Ltd. Mumbai

    3.  Recovery of Co and Ni values from scrap, 2025 MIDHANI, Hyderabad

    4.  Recovery of Co from impure Co hydroxide cake, 2025 MIDHANI, Hyderabad

    5.  Recovery of Electrolytic Manganese Dioxide (EMD) from Manganese Ore: Process optimization for existing plant at MOIL, alternate process development and Basic Engineering Package preparation, 2022, MOIL, Nagpur

    6.  Recovery of tungsten from scrap and Hutti gold mine tailings, 2020 DMRL (DRDO),

    7.  Hyderabad

    8.  Recovery of alumina, silica and iron values from Indian fly ash, 2019, National Aluminium Company (NALCO), Bhubaneswar

    9.  Splitting of sodium sulphate bearing effluent through electro-membrane process for the production of sodium hydroxide and sulphuric acid, 2017, M/s Heavy Water Board, Mumbai

    10. Recovery of Pd from spent nuclear fuel effluent (high-level liquid waste) using ionic liquids, 2015, Indira Gandhi Centre for Atomic Research (IGCAR), Kalpakkam

    11. Recovery of high pure Te, Cu and Pb from anode slime, 2012, M/s Hindalco Industries Ltd., Dahej, Gujarat.

    12. Electrochemical reduction cell assembly design.          , 2008 M/s Heavy Water Board, Mumbai

    13. Chromite recovery from COB plant tailings and sub-grade chromite ore, 2008, M/s Jindal Stainless Steel Limited, Bhubaneswar

    14. Recovery of Ni and Co from Chromite Overburden (COB) through reduction roasting-ammoniacal leaching route, 2003, CSIR, Hindustan Zinc Ltd., GTZ- Germany

    15. Recovery of Cu, Ni and Co from polymetallic nodules through ammonia- ammonium sulphate-sulphur dioxide leaching route, 2000, Ministry of Earth Sciences, New Delhi

    16. Recovery of cobalt carbonate from cobalt bearing slag of South Africa, 1998, M/s Shalina Trading Corporation Ltd., Mumbai

    17. Recovery of cobalt from super alloy scrap/sludge., 1997, M/s Rubamin Ltd., Baroda

    18. Production of Copper cathode from secondary sources, 1997, M/s Hydromet India Ltd, Kancheepuram